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簡(jiǎn)體中文 ?????? ??????? ???????? ??? ???? ???? ?? ???????? ??????????? ????????? ?????? ???? ?????. ?? ??????? ??????? ? ???? ?????? ???? ????? ?????? ??????? ? ????? ?????? ?? ??????? ??????? ????????? ?????? ?????? ?? ???????? ????? ???????? ?? ???? ????? ?????? ??????? ???????? ????? ?????? ????????. ???? ???? ???????? ???? ???? ??????? ??????? ???????? ??? ??????? ????????? ??? ????? ?????? ?? ?????????? ??? ????? ?? ???????. ???? ??? ???? ?????? ?? ??? ???????? ??????? ????? ???????? ????. ????????? ???????? ?????? ?????: ????? ??????? ?????????? (SEM) ??????? ?????????? ??????? (TEM) ?????? ?????????? ????? (SEM) ????? ??? ????? ?????? ???? ???????? ????? ?? ?????? ???? ???????? ?????? ?? ??? ???? ?? ????????? ??? ??? ???????? ? ??? ?????? ?????? ?????? ?????? ????? ??????? ???????? ? ??????? ?? ?????? ???? ???????? ???? ??????? ??????? ???? ????????. ?? ?????? ???? ????? ?? ??? 1965. ??? ?????? ???? ????? ??????? ??????? ??????? ??????????? ??????? ??? ??? ?????? ? ?? ???????? ???? ????????? ???? ???? ???? ?????? ? ?? ???? ???? ????????? ?????? ?????? ???? ??? ??????? ?????? ? ????? ?? ?????? ?????? ????????? ??????? ??????. ???? ????? ??????? ?????????? ?? ????? ??? ???????? ?????? ???? ???????? ???? ? ???????? ??? ?????? ????? ?????? ???????? ?????. ??? ?? ???? ?????? ???? ?????? ????? ?????? ? ?????? ????? ??? ?? ??? ???? ???? ??? ?????? ???????? ???? ?? ????. ??? ?? ???? ?? ????? 1 ? ? ????? ????? ???? ????? ?????????? ????? ???? ???? ???? ???? ??????????? ???. 1: (?) ?????? ????? ????? ??????? ?????????? (SEM) ? (?) ????? ???? ?? ?????? ????? ?? ???? ?????? SEM (????? TiO2 ????????) 1.1 ???? ?????? ?????????? ???? SEM: ??? ?? ???? ?? ????? 1 ? ? SEM ?? ??????? ??? ???? ????????? ???? ?????? ? ??? ????? ?? ????????? ?????? ??? ?????? ??????? ? ?????????? ??????? ?? SE ???????? ? ???? ????????? ???? ?????? SE ? ???????? ???? ????? ?? ????? ????? ? ???????? ??? ???????. ???? ?????? ??????? (3) ??? ???? ? 30 ??? 40 ???? (4) ???? ?? ????? ??????? ???????? ?? 4 ???? ??? 150.000 (5) ???? ?????? ??????? ??????? ????? ??????? ??????? ??????? 1.3 ?????? ???????: ???????? ????????? ??????? ??????? ???? ???????? ??????. ?? ???? ?????? ???? ??? ???? ???? ???? ??? ????????. ??? ???????? ???? ????? ??????? ?????? ?????? ?????? ? ????? ????? ??????? ? ????? ????? ??????? ???????. ???? ?? ???? ???? ???? ????? ?????? ?????? ??? ???????? ?????? 2. ????? 2: (?) ??????? ??????? ????? ???????? ???? ?????? TEM ? (?) ???? ?????? TEM (???? ?????? ?? Co3O4) 2.1 ??????: ??? ??????? ???? ????????? ?????? ?????? ??? ?????? ?????? ????? ????????? ???? ?????? ?????? ??????. ??? ??? ??? ??????? ??? ???? ?????? ??? ??????? ?????? ???? ????????? ?????? ????????? ? ???? ????? ?????? ??????? ?? ??? ?????. 2.2 ???????: (1) ???? ????? ? h <1000 ? (2) ???? ?????? ?????? ??????? ? ????? ???? ???? (3) ??? ????? ? ???? ?? 2 (4) ????? ???? ???? 2-3 ?????? ???????: ??? ????? ?????? ???????? ????????? ?? ??????? ??? ?????? ???????? ??? ????????? ? ???????? ?????? ??????? ????? ????. ???????? ???????? ?? ?????? ??????? ???????? ??????. ???? ?????? ?????????? ???? ????? ??????? HRTEM ?? ????? ?????? ???????? ???????? ??????? ??????. ??? ?? ???? ?? ????? 2 ? ? ??? ?????? ?????? ??????? ????? ??????? ?? ????? ???? ? ?? ???? ????? ????? ??????? ??? SEM ? ???? ?? ??? ???? ? ???? ?????? ????? ???? ??? ? ????? ?? ????? HRTEM ????? ??? ????? ??????? ?????? ? information.3 ?????. ?????? ??????? ??????? ??????: ????? ???? ?????? ??????? (XRD) ????? ???? ?????? ??????? (XRD). ?? ???? ???? ?????? ??????? ?????? ? ?????? ??? ?????? ? ?????? ??? ????? ?????? ? ?????? ???????? ?? ??????? ??????? ?? ?????????? ?????? ???? ??? ????????? ??????. ????? ???? ?????? ??????? ?? ??????? ???????? ?????? ????? ??????? ???????? ??????. ????? ???? ???? (?????? ?? ??? ??????) ?????? ???????? ? ??? ????? ?????? ??????? ??????? ?????? ????? ?????? ?? ????????. ???? ??????? ?????? ??????? ??????? ???? ?????? ???????? ??????? ???????? ????? ??????. ??? ?????? ??????. ????? ????? ???? ?????? ??????? ?????? ??? ????? ?????? ? ???? ?????? ? ??????? ? ???? ?????? ??????? ? ????? ????? ?? ????????? ??? ????? ???????. ???? ? ?? ??????? ????? ???? ?????? ??????? ?????? ???? ???? ?????? ???? ?????? ???????? ??? ???? ???? ?? ????? ???????? ?? ????? ????????. ????? 3: (?) ??? XRD ????? ???????? ???? ? (?) ?????? ??????? ?????? ???? ?????? ??????? 3.1 ???? XRD: ????? ????? ???? ?????? ??????? ?? ????? ????? ????????????? ? ????? ?????? ?????? ?????? ???????? ?? ???????. ????? ????? ?????? ?? ???? ?????. ???? ??????? ????????? ???????? ?? ???? ?? ??? ?????? ??????? ??????. ????? ??? ?????? ????? ???? ???? ?? ??????? ? ????? ????? ??? ????? ??? ??? ??????? ??????? ????????? ? ????? ????? ??? ??????? ??????? ?? ??? ??????? ?????? ?????? ????? ????? ?????? ????? ????? ?? ??? ????????? ? ??? ???? ??? ????? ????????. ????? ????? ?????? ???? ?? ????? ?????? ? ??? ??? ??? ???????? ??????? ???? ?? ???? ? ????? ?????? ??????? ??????? ? ???? ???? ????? ????? ?????. ???? ????? ? ??? ????? ????? ???? ?????? ?? ??? ?????? ?? ???? ??? ???? ?????? ?????? ????????. ??? ????? ??? ???? ?????? ??? ??? ?????? ??????? ?? ???? ??????. ???????? ?????? Bragg: 2dsinθ = nλ ? ?????? ?????? ??? ???? ????? ?????? ????? ?????? ???????? ????? ????? ?????? ?????? ????? ?????? θ ???? ? ?? ??? ????? ????? ??? ????? PDF 3.2 ????? ?????? XRD: ????? ???? XRD ?? ?????? ????? ????? ????? ?? ?????? ????? ?????? ??????? ??????? ?? ?????? ???????? ?? ?????? ??????????? ? ??? ????? ???????? ?????? ???????? ?????? ??????? ???????? ???????. ??? ???? ?????? ??????. ?? ???? ????????? ??? ????? ?? ???? ???????? ? ?? ???? ????? ?????? ???????? ??????? XRD ??????? ????? ??????? ??????. ???? ????? 3 ? ??? XRD ??????? ????? ???????? ???? Co3O4. ??? ????? ??????? ??????? ??????? ?????? ??? ????? ????? ?????? PDF ????????. ???? ??????? ????? ?????? ??????? ???????? ?? ??? ????? ???? ?????? ?????? ? ??? ???? ??? ?? ??????? ??? ???? .3.3 ??????? ?????? ????? ???????: ????? ????? ?? ????? ????? ???? ????. ????? ????? ??????? ????? ? ???? ????? ??? ?????? ? ??? ???? ?? ????? ????? ?????? ???????. ?????? ????????????? (CV) ???? ?????????? ?????? ?????? ?????? ???????? ?????? ????? ???? ?????? ???????? ??? ?????? ????????????? ? ??? ??? ????? ?????????? ?????????????? ??????. ?????? ?????? ???????: ????? ??? ???????????? ????? ?????????. ????? ??????? ?? ??????? ????? ??????? ?????? ????? ?????? ???? ????? ?????? ?????? ?????? ??? ????? ?? ???? ????? ?????. ?????? ??????? ?? ????? ??????? ?????? ?????? ?????? ???????? ??? ????? ?????? ????? ????? ??????. ????? ???? ??????? ? ???? ????? ??? ???? ?????? ????? ????? ????????? ? ???????? ?????? ?????? ??????? ?? ??????? ?? ????? ????? ????? ? ?????? ??????? ????????? ???????. ??????? ???? ???? ????? ?????? ????? ????? ? ?????? ????? ?????? ????? ??????? ? ??????? ??????? ???? ???? ?? ???? ???? ???? ????? ??????? ?????? ? ???? ???????. ??????? ?????? ????????????? ?????? ? ?????? ?? ???? ??????? ??????? ??????? ?? ???? ?????????? ?????? ? ????? ???? ??????? ???? ???? "??????? ?????? ?????????????". ???????? ??? ??????? ??????? ?????????? ???????? ? ???? ?? ?????? ??? ??????? ????? ???????? ?????? ???????? ??????? ???????? ?????????? ??????? ???????? ?? ????? ??????? ???????? ?????????? ??????? ?????????. . ??????? ?????? ????????????? ?????? ? ??? ??????? ??????? ??????? ?????? ?? ???? ???? ?????????? ??????. ????? ????? ?????? ?? ??????? ???????? ? ??????? ??? ??????? ?????? ??????? ?????? ??????? ?? ?????? ??????? ?????. ????? 4: (?) ???? ???? ?????? ??????? ????? ????????? ?????? ???????? ? (?) ?????? ????? ???????? ????? ?????? ??????? ???????? ?????? ????? ???????? ??????? ?????? ???????: ??? ????? ?????? ???????? ?? ???????? ???????? ? ???? ????? ???????? ??????? ???? ??????. ?????? ?? ?????? ????? ????? ?????? ????? ????? ????? ??????????????? ? ???????? ???????? ?????? ???? ???? ? ???? ?? ????? ?? ???? ????? ??????? ? ????? ??????? ??????. ???? ????? ?? ????? ???????? ???? ???? ????????? ?? ?????????: Wuhan Blue Power ? Shenzhen Xinwei. ??? ????? ?????? ???? ? ???? ?????? ???? ???? ????????. ????? 4 ? ?? ???? ???? ??????? ?? ??????? ???????? ???????. ?????? ?? ??? ??? ???? ????? ?????? ??????? ??????? ???? 60 ????? ? ????? ????? ???? NS ??????? ??? 150 ?????. ??????: ???? ?????? ?? ?????? ???????? ????? ?????? ????????. ?????? ?????? ?? ?????? SEM ? TEM ? XRD ??????? ??????? ??????? ???????? ?????. ???? ????? ??????? Raman (Raman) ? ???????? ?????? ??????? ??? ??????? (FTIR) ? ???????? ?????? ????????? ?????? ??????? ??????? (XPS) ? ?????? ??? ?????? (EDS) ??????? ?????? ?????????? ? ???????? ?????? ?????? ???? ????????? (EELS) ?????? ??? ???????? ??????? ? ????????. ???? ?????? ????? ????? BET. ???? ??????? ??????? ?????? ???????? ??????? ?????????? (XAFS) ?? ??? ???????. ?? ??????? ???????? ??????? ? ????? ????? ??????? ???????? ????? ???????? ???????? ????? ?????? ????????? ??? ????? ???????? ?????????? ?? ???????? ?????? ?????? ??????. ?????? ????? ??? ??????? ?????? ???? ?? ??????? ????? ??? ??? ?? ????? ?????? ?????? ?? ???? ??????? ????????.
??????: Meeyou Carbide
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